technology of synthetic resins & emulsion polymers (hand book)

technology of synthetic resins & emulsion polymers (hand book)
Author: Dr. Himadri Panda
ISBN: 9788189765965
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TECHNOLOGY OF SYNTHETIC RESINS & EMULSION POLYMERS

THE CHEMISTRY OF RESIN FORMATION AND RESIN PROPERTIES


Introduction
Fundamentals of Polymer formation
Functions of Reactive Groups
Cross -linked Polymers
Formation of Polymers
Polycondensation
Interfacial Polycondensation
Sequence of Reaction
Copolymer Formation
Rate of Polymerization
Addition Polymerization in Practice
Chain Transfer Reactions
Strereopsecific Polymerization
Polyaddition Reactions
Types of Polymers
Polyesters
Formation of Alkyds
Saturated and Unsaturated polyesters
Polyamides
Phenolic Resins
Amino Resins
Epoxide Resins
Vinyl Polymers
Polyvinyl Alcohol
Silicones
Practical Applications

THE CHEMICAL ENGINEERING OF OIL AND RESIN PROCESSING

General Requirements for Processing Equipments
Materials of Construction
Branches and Connections
Stirring Equipment
Types of Agitators
Sealling
Drive Units
Fume Disposal and Scrubbing
Desing Consideration
Sludge Handling Equipment
Condensing and Refluxing
Design and Layout of Tubes
Water Receiver
Ancillary Equipment
Agitators
Heating
Reflux Condenser
Thermometer
Steam Arrangements
Vacuum Pumps
Pressure and Flow Indication
Fume Extraction
Lagging
Miscellaneous
Heating and Cooling
Criteria for Selection of Heating and Cooling system
Calculation of Film Coefficients
Heat Transfer Coefficient
Steam Heating
Pressurised Hot Water
Heating at Higher Temperature
Direct Firing
Immersion Tubes
Kestner Coil
Typical Arrangement
Cooling
The advantages of this type of heating system are
Heating by Electricity
Immersion Heating
Heating through The Vessel Wall
Induction Heating
Isoductive Heating System
Heating of Pipework and Ancillaries

ALKYD RESINS

The nature of Alkyd Resin
Raw Materials
Dibasic Acids
Polyhydric Alcohols
Modifier for Alkyd Resins
Formulation of Alkyd Resins
Formula Development
Calculation of Alkyd Formulations
Typical Formulations
Manufacture of Alkyd Resin
Alcoholysis
Catalysts
Control of Alcoholysis
Acidolysis
Fatty Acid Process
Esterification
Alkyd Manufacturing Plant
Applications of Alkyd Resins
Oil Froe Alkyds

POLYESTER

Saturated Polyesters
Condensation and Addition Polymerization
Main Components of Unsaturated Polyesters
Brief History of Surface Coatings
Characteristics of Unsaturated Polyesters
Two points should be noted here
Functions of Initiators Accelerators, Inhibitors
Effect of structure of Polyester Backbone on Properties of Cured products
Effect of Chemical structure on Melting points of Linear Polyesters
Effect of Structure on Properties of Cured Products
Commonly used polyols and their advantages are
The effect of unsaturated monomers on properties of cured products
Polyester coating composition
Radiation Cure
Methods of Application

AMINO RESINS

Formation of Amino Resins
Methylol formation
Alkylation
Urea Formaldehyde Resins
Methylol Formation
Etherification reaction
Melamine Formaldehyde Resin
Melamine Methyl Formation
Alkylation of Melamine Methylots
Other Amino Resins
Glycoluril
Production Amino Resins
Properties of Amino Resins
Uses of Amino Resins
Self Polymerization
Co reaction with alkyd and polyester resins
Co-reaction with Acrylic Resins
Epoxy resins
Acid Catalysed Lacquers
Water based Coatings
Appendix 1 Solvent Tolerance
Appendix 2 NonVolatile Content

POLYURETHANE RESINS

Chemistry
Raw Materials
Isocyanates
Toylene Diisocyanate (TDI)
4,4' Diphenylmethane Diisocyanate (MDI)
Hydroxyl Component
Hazards of Isocyanates Classification of Polyurethanes
Urethane Oils and Urethane Alkyds
Moisture cured urethanes
Blocked Isocynatiee Systems
Two component catalyst cured Polyurethanes
Two component Polyol Type Polyuethanes

EPOXY RESINS

Epoxy Resins Manufacture and  Characterization
Curing Agents for Epoxy Resins
Principles n Formulating with Epoxy Resins
Solventless and High Solids Coatings
Tar Epoxy Coatings
Flooring Compounds
Fibreglass Laminates
Solvent based Paint
High Solids Coatings
Solventless Tar Epoxy Coatings
Solventless Coating for Airless Spray Equipment
Single Pack Epoxy Maintenance Paints
Epoxy Esters
Single Pack Thermoplastic Epoxy Systems
Epoxy Industrial Baking Finishes

WATER DISPERSIBLE EPOXY RESINS

Epoxy/Polyamide Emulsions
Epoxy Baking Enamels
Water Dispersible Epoxy
Resin Coatings for Electrodeposition
Epoxy Aqueous Powder Suspension (APS)

SILICONE RESINS

Direct Process
Grignard Process
Preparation of Silanots
Polymerization
Silicone resins
Pure Silicone Resins
R:Si Ratio
Methyl and phenyl content
Viscosity
Properties of pure Silicone
Surface Coating Resins
Resistance to Weathering
Bending Resins
Silicone Intermediates
Silicone Organic Copolymers
Preparation and Formulation of Silicone Resin Based Coatings
Cure Catalyst Driers
Pigments and Dyes
Thinners
Application Guides
Surface Preparation
Priming
Applying the Coatings
Curing
Uses
Toxicity
Other Silicone Resin
Application
Electrical Varishes
Release Resins
Masonry Water Repellants
other Silicones for Surface Coatings

ACRYLIC SOLUTION RESINS

Backbone Monomers
Synthesis
Addition Polymerization
Copolymerization
Thermoplastic Acrylic
Solution Polymerization
Properties and End Uses
Thermosetting Acrylics
Selection of Monomer
Classification and properties
Acrylamide Copolymers
Acid Copolymers
Hydroxy Copolymers
Curing Reactions
Aqueous Solution Acrylics
Non Aqueous
Dispersions (NAD)

RUBBER RESINS

Introduction
Natural Rubber
Synthetic Rubbers
Procedure
Rubber Resins and Latexes
Chlorinated Rubber Resins
Lifting
Parlon
Cyclized Rubber Resins
High Styrene Butadiene
Rubber Resins
Chrolorinated Biphenyls
Chlorinated Paraffins
Synthetic Rubber Resins Latexes

EMULSION POLYMERS

Key Components in Emulsion Polymerization
Surfactants
Initiators
Water
Polymerization in Emulsion Systems
Based on Styrene
Influence of Monomer Componsition of roperties and performance
Hardening Monomers
Vinyl Acetate
Styrene
Methyl Methacrylate
Flexibilizing Monomers
Esters of Acrylic Acids
Esters of Maleic or Fumaric Acids
Vinyl Esters
Olefins-Butadiene
Olefins-Ethylene
Specific Monomers
Effect of Monomer Composition on Film Properties
Effect of Water Phase and Particle Size
Particle Size
Manufacture and Testing
Process Variables
Emulsion Testing
Application of Emulsion Polymers
Adhesive Industry
The Printing Ink Industry
The Printing Ink Industry
The Textile Industry
The Leather Industry
The Floor Polish Industry
The Paper Industry
The Agriculture Industry
Soluble Alkyds
Disadvantages are
Polyesters
Silicone modified Alkyds and Polyesters
Epoxy Resins
Anhydrides
Defunctioalizing the Epoxide Ring
Cationic Polymers
Thermoplastic Polymers
Thermosetting Polymers
Amino Resins
Urea Formaldehyde
Melamine Formaldehydes
Substituted Guanamine Formaldehyde
Self cross linking
Other Water soluble Polymers
Viscosity Characteristics
Amines
Viscosity
Drying
Stability
Foam Control
Colour Retention
Toxicity
Variation of Amine Levels
Viscosity
Drying Properties
Stabilit
Gloss
Cosolvents
Coupling Efficiency
Viscosity
Variation of Cosolvent water ratio
Stability
Drying properties
Foam Control
Drier for air dry and Force dry systems
Cross Linking os water Soluble coatings
Additives for Coatings
Pigments
Formulation of Water Soluble Coatings
Trouble Shooting with Water Soluble Polymers

WATER SOLUBLE POLYMERS

Classification
Properties of Cellulose Ethers
Application
Uses


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